By Magrone P., Servadei R.
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Additional info for A stability result for mountain pass type solutions of semilinear elliptic variational inequalities
Wt. 06 Synthesis -Preparation by reaction of 20% aqueous titanium trichloride solution on the 5-bromo-2-hydroxy-3-nitroacetophenone in toluene, at room temperature, in a sealed tube [505, 1190], (31%) . p. 99-102° [505,1190]; Spectra (NA). wt. 52 -Preparation by reduction of 3-bromo-2-hydroxy-5-nitroacetophenone with an excess of tin in concentrated hydrochloric acid at 100° (82%) . p. 200°(d) ; Spectra (NA). l-(3-Amino-5-chloro-2-hydroxyphenyl)ethanone [21312-85-6] C8H8CINO2 molwt.
22 Synthesis -Preparation by reaction of 2 N aqueous sodium hydroxide on the 2-dimethylcarbamylthio-6-hydroxyacetophenone in refluxing methanol (65%) . p. and Spectra (NA). wt. 22 Synthesis -Preparation by reaction of stannous chloride dihydrate on the 3-(chlorosulfonyl)-4-hydroxyacetophenone with gaseous hydrochloric acid in acetic acid at 25-30° (31%) [1154,1385]. p. 117-120° [1154,1385]; Spectra (NA). Previous Page l-(2,3-DihydroxyphenyI)ethanone [13494-10-5] C8H8O3 molwt. 15 Syntheses -Preparation by reaction of acetic anhydride on the pyrocatechol with 70% perchloric acid on a steam bath (58%) , at 100° (4%) .
With titanium tetrachloride (11%) . -Obtained by reaction of acetyl chloride on the phenyl borate with aluminium chloride in refluxing carbon disulfide (54%) . -Obtained by reaction of acetic anhydride on the phenol, using a steam bath, *with 70% HClO 4 (51%) . *with aluminium chloride (38%) . *with zinc chloride at 145-150° (36%) . -Obtained by reaction of acetylacetone on the phenyl benzoate with aluminium chloride in nitrobenzene, at 45° (3%) . -Preparation by diazotization of 2-aminoacetophenone and hydrolysis of the diazonium salt obtained [96,517,1441].